TA Instruments

AR1757-0001f

15/03/2013 16:01:20

Sample name	DI Blank 25 mm AL
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1757
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 16:01:20

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0120	5.906	-40.887	10000	20.0	6.095	31.012	-13.33	7.383	-1.805	24830	5.2952	455.6	6.6190	661.90	3.411E-3	0.0	0.5
2.0120	9.771	11.215	10000	20.0	6.098	32.012	3.656	12.21	0.2993	24850	13.1288	166.6	16.411	1641.1	3.411E-3	0.0	0.5
3.0120	15.45	21.809	10000	20.0	6.101	33.012	7.109	19.31	0.3681	24860	26.8347	66.63	33.543	3354.3	3.411E-3	0.1	0.6
4.0120	18.39	28.410	10000	20.0	6.099	34.012	9.260	22.99	0.4027	24850	40.9562	47.00	51.195	5119.5	3.411E-3	0.1	0.6
5.0120	24.64	44.020	10000	20.0	6.097	35.012	14.35	30.80	0.4658	24840	68.4024	26.18	85.503	8550.3	3.411E-3	0.1	0.6
6.0120	31.55	65.069	10000	20.0	6.098	36.012	21.21	39.43	0.5378	24850	106.4170	15.98	133.02	13302	3.411E-3	0.1	0.6
7.0120	33.99	72.651	10000	20.0	6.098	37.012	23.68	42.49	0.5573	24840	126.2380	13.76	157.80	15780	3.411E-3	0.1	0.6
8.0120	39.27	91.088	10000	20.0	6.093	38.012	29.69	49.09	0.6048	24830	165.0110	10.30	206.26	20626	3.411E-3	0.1	0.6
9.0120	46.01	115.99	10000	20.0	6.085	39.012	37.81	57.51	0.6575	24790	223.1750	7.497	278.97	27897	3.411E-3	0.2	0.7
10.012	50.93	136.46	10000	20.0	6.085	40.012	44.48	63.66	0.6986	24790	274.9650	6.117	343.71	34371	3.411E-3	0.2	0.7
11.012	55.70	156.44	10000	20.0	6.082	41.012	50.99	69.62	0.7324	24780	325.7890	5.112	407.24	40724	3.411E-3	0.2	0.7
11.996	60.07	176.84	10000	20.0	6.073	41.996	57.64	75.09	0.7676	24740	377.2880	4.388	471.61	47161	3.411E-3	0.2	0.7
13.012	64.39	196.54	10000	20.0	6.072	43.012	64.06	80.49	0.7960	24740	434.7080	3.819	543.39	54339	3.411E-3	0.2	0.7
14.012	69.13	221.48	10000	20.0	6.068	44.012	72.19	86.41	0.8355	24730	498.9400	3.312	623.68	62368	3.411E-3	0.2	0.7
15.012	75.66	255.11	10000	20.0	6.059	45.012	83.15	94.58	0.8792	24690	593.8980	2.760	742.37	74237	3.411E-3	0.3	0.8
16.012	79.91	277.24	10000	20.0	6.062	46.012	90.37	99.89	0.9047	24700	664.7180	2.475	830.90	83090	3.411E-3	0.3	0.8
17.012	84.51	304.99	10000	20.0	6.050	47.012	99.41	105.6	0.9411	24650	740.2590	2.209	925.32	92532	3.411E-3	0.3	0.8
18.012	90.96	340.26	10000	20.0	6.045	48.012	110.9	113.7	0.9754	24630	854.6980	1.905	1068.4	1.0684E5	3.411E-3	0.3	0.8
19.012	95.02	362.49	10000	20.0	6.046	49.012	118.2	118.8	0.9948	24630	930.8360	1.746	1163.5	1.1635E5	3.411E-3	0.3	0.8
19.996	99.38	392.74	10000	20.0	6.037	49.996	128.0	124.2	1.031	24600	1020.2400	1.594	1275.3	1.2753E5	3.411E-3	0.3	0.8
21.012	105.8	430.93	10000	20.0	6.031	51.012	140.5	132.3	1.062	24570	1153.2000	1.405	1441.5	1.4415E5	3.411E-3	0.4	0.9
22.004	109.9	453.32	10000	20.0	6.022	52.004	147.8	137.4	1.076	24530	1241.8600	1.300	1552.3	1.5523E5	3.411E-3	0.4	0.9
22.996	114.2	482.08	10000	20.0	6.016	52.996	157.1	142.8	1.101	24510	1343.2900	1.202	1679.1	1.6791E5	3.411E-3	0.4	0.9
24.012	120.6	530.81	10000	20.0	6.010	54.012	173.0	150.8	1.147	24490	1495.3400	1.077	1869.2	1.8692E5	3.411E-3	0.4	0.9
25.024	124.7	555.07	10000	20.0	6.004	55.024	180.9	155.9	1.161	24460	1596.6200	1.006	1995.8	1.9958E5	3.411E-3	0.4	0.9
26.012	129.0	589.20	10000	20.0	5.993	56.012	192.0	161.3	1.191	24420	1710.8300	0.9385	2138.5	2.1385E5	3.411E-3	0.4	0.9
27.012	135.4	636.69	10000	20.0	5.987	57.012	207.5	169.3	1.226	24390	1881.6400	0.8510	2352.1	2.3521E5	3.411E-3	0.5	1.0
28.012	139.5	664.67	10000	20.0	5.981	58.012	216.6	174.4	1.242	24370	1995.5300	0.8009	2494.4	2.4944E5	3.411E-3	0.5	1.0
29.016	143.6	695.68	10000	20.0	5.972	59.016	226.8	179.6	1.263	24330	2115.7700	0.7547	2644.7	2.6447E5	3.411E-3	0.5	1.0
30.012	150.0	736.82	10000	20.0	5.963	60.012	240.2	187.5	1.281	24290	2305.6001	0.6907	2882.0	2.8820E5	3.411E-3	0.5	1.0
30.996	154.1	775.13	10000	20.0	5.960	60.996	252.7	192.7	1.311	24280	2432.0100	0.6541	3040.0	3.0400E5	3.411E-3	0.5	1.0
31.996	158.3	806.66	10000	20.0	5.951	61.996	262.9	197.8	1.329	24250	2565.3201	0.6197	3206.7	3.2067E5	3.411E-3	0.5	1.0
33.012	164.6	854.59	10000	20.0	5.940	63.012	278.6	205.8	1.353	24200	2774.4299	0.5714	3468.0	3.4680E5	3.411E-3	0.6	1.1
34.012	168.8	885.71	10000	20.0	5.934	64.012	288.7	211.0	1.368	24180	2912.4900	0.5432	3640.6	3.6406E5	3.411E-3	0.6	1.1
35.012	174.9	930.31	10000	20.0	5.921	65.012	303.2	218.6	1.387	24120	3129.0100	0.5048	3911.3	3.9113E5	3.411E-3	0.6	1.1
35.996	179.1	974.21	10000	20.0	5.911	65.996	317.5	223.9	1.418	24080	3278.9700	0.4805	4098.7	4.0987E5	3.411E-3	0.6	1.1
36.996	183.3	1009.4	10000	20.0	5.898	66.996	329.0	229.1	1.436	24030	3430.5200	0.4580	4288.2	4.2882E5	3.411E-3	0.6	1.1
37.996	189.3	1074.6	10000	20.0	5.886	67.996	350.3	236.6	1.480	23980	3658.6699	0.4283	4573.3	4.5733E5	3.411E-3	0.6	1.1
38.996	193.5	1106.4	10000	20.0	5.877	68.996	360.6	241.8	1.491	23940	3822.0200	0.4094	4777.5	4.7775E5	3.411E-3	0.6	1.1
39.996	199.7	1162.3	10000	20.0	5.867	69.996	378.9	249.6	1.518	23900	4068.9199	0.3837	5086.2	5.0862E5	3.411E-3	0.7	1.2
40.996	203.7	1186.9	10000	20.0	5.861	70.996	386.9	254.6	1.519	23880	4234.9800	0.3683	5293.7	5.2937E5	3.411E-3	0.7	1.2
42.012	210.0	1237.0	10000	20.0	5.849	72.012	403.2	262.4	1.536	23830	4499.4199	0.3460	5624.3	5.6243E5	3.411E-3	0.7	1.2
43.012	214.1	1298.5	10000	20.0	5.841	73.012	423.2	267.6	1.582	23800	4677.6699	0.3323	5847.1	5.8471E5	3.411E-3	0.7	1.2
44.016	218.1	1336.8	10000	20.0	5.833	74.016	435.7	272.7	1.598	23760	4851.6401	0.3197	6064.6	6.0646E5	3.411E-3	0.7	1.2
45.016	224.3	1383.7	10000	20.0	5.821	75.016	451.0	280.3	1.609	23720	5129.8101	0.3018	6412.3	6.4123E5	3.411E-3	0.8	1.3
46.012	228.4	1429.9	10000	20.0	5.812	76.012	466.1	285.5	1.632	23680	5317.8701	0.2905	6647.3	6.6473E5	3.411E-3	0.8	1.3
47.012	234.5	1474.6	10000	20.0	5.798	77.012	480.6	293.1	1.640	23620	5601.8799	0.2749	7002.4	7.0024E5	3.411E-3	0.8	1.3
48.012	238.5	1536.3	10000	20.0	5.766	78.012	500.8	298.1	1.680	23490	5797.3398	0.2643	7246.7	7.2467E5	3.411E-3	0.8	1.3
49.004	242.7	1562.7	10000	20.0	5.781	79.004	509.4	303.4	1.679	23550	5999.2402	0.2559	7499.1	7.4991E5	3.411E-3	0.8	1.3
50.012	248.8	1631.9	10000	20.0	5.768	80.012	531.9	310.9	1.711	23500	6303.4600	0.2431	7879.3	7.8793E5	3.411E-3	0.8	1.3
51.012	252.8	1667.2	10000	20.0	5.757	81.012	543.4	316.0	1.720	23450	6510.1001	0.2349	8137.6	8.1376E5	3.411E-3	0.9	1.4
52.012	259.0	1740.1	10000	20.0	5.735	82.012	567.2	323.8	1.752	23360	6831.9600	0.2229	8540.0	8.5400E5	3.411E-3	0.9	1.4
53.012	263.1	1772.1	10000	20.0	5.729	83.012	577.6	328.9	1.756	23340	7046.2500	0.2158	8807.8	8.8078E5	3.411E-3	0.9	1.4
54.012	269.1	1833.5	10000	20.0	5.715	84.012	597.6	336.4	1.776	23290	7376.2100	0.2058	9220.3	9.2203E5	3.411E-3	0.9	1.4
55.012	273.3	1873.7	10000	20.0	5.696	85.012	610.7	341.6	1.788	23210	7601.2900	0.1989	9501.6	9.5016E5	3.411E-3	0.9	1.4
55.996	277.3	1951.9	10000	20.0	5.690	85.996	636.2	346.7	1.835	23180	7828.1099	0.1929	9785.1	9.7851E5	3.411E-3	0.9	1.4
57.012	283.4	1999.2	10000	20.0	5.677	87.012	651.6	354.3	1.839	23130	8169.8398	0.1843	10212	1.0212E6	3.411E-3	1.0	1.5
58.012	287.5	2029.4	10000	20.0	5.661	88.012	661.5	359.3	1.841	23060	8408.3096	0.1786	10510	1.0510E6	3.411E-3	1.0	1.5
59.012	293.6	2105.9	10000	20.0	5.657	89.012	686.4	367.0	1.870	23050	8767.7803	0.1712	10960	1.0960E6	3.411E-3	1.0	1.5
60.012	297.6	2150.3	10000	20.0	5.634	90.012	700.9	372.0	1.884	22950	9006.8799	0.1659	11259	1.1259E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	300.0	2175.2	10000	20.0	5.630	92.000	709.0	375.0	1.891	22940	287.7040	0.1631	359.63	35963	3.411E-3	0.0	1.5
2.0000	300.0	2188.0	10000	20.0	5.636	93.000	713.2	375.0	1.902	22960	542.2980	0.1633	677.87	67787	3.411E-3	0.0	1.6
3.0000	300.0	2185.6	10000	20.0	5.625	94.000	712.4	375.0	1.900	22920	915.9860	0.1629	1145.0	1.1450E5	3.411E-3	0.1	1.6
3.9960	300.0	2179.4	10000	20.0	5.644	94.996	710.4	375.0	1.894	22990	1167.4000	0.1635	1459.3	1.4593E5	3.411E-3	0.1	1.6
5.0000	300.0	2180.8	10000	20.0	5.622	96.000	710.8	375.0	1.896	22910	1418.6600	0.1629	1773.3	1.7733E5	3.411E-3	0.1	1.6
6.0040	300.0	2181.8	10000	20.0	5.624	97.004	711.1	375.0	1.896	22910	1795.8700	0.1629	2244.8	2.2448E5	3.411E-3	0.1	1.6
7.0000	300.0	2191.0	10000	20.0	5.635	98.000	714.2	375.0	1.904	22960	2047.1899	0.1633	2559.0	2.5590E5	3.411E-3	0.1	1.6
8.0040	300.0	2176.3	10000	20.0	5.623	99.004	709.4	375.0	1.892	22910	2428.6899	0.1629	3035.9	3.0359E5	3.411E-3	0.1	1.7
9.0000	300.0	2185.8	10000	20.0	5.626	100.000	712.5	375.0	1.900	22920	2675.4399	0.1630	3344.3	3.3443E5	3.411E-3	0.2	1.7
9.9960	300.0	2179.3	10000	20.0	5.634	100.996	710.3	375.0	1.894	22960	2926.6899	0.1633	3658.4	3.6584E5	3.411E-3	0.2	1.7
11.000	300.0	2174.9	10000	20.0	5.645	102.000	708.9	375.0	1.890	23000	3303.6399	0.1636	4129.6	4.1296E5	3.411E-3	0.2	1.7
11.996	300.0	2182.0	10000	20.0	5.640	102.996	711.2	375.0	1.897	22980	3555.0000	0.1634	4443.8	4.4438E5	3.411E-3	0.2	1.7
12.996	300.0	2176.6	10000	20.0	5.654	103.996	709.4	375.0	1.892	23040	3808.1201	0.1638	4760.2	4.7602E5	3.411E-3	0.2	1.7
13.996	300.0	2216.3	10000	20.0	5.635	104.996	722.4	375.0	1.927	22960	4186.4102	0.1633	5233.0	5.2330E5	3.411E-3	0.2	1.7
15.000	300.0	2199.3	10000	20.0	5.632	106.000	716.9	375.0	1.912	22950	4434.6499	0.1632	5543.3	5.5433E5	3.411E-3	0.3	1.8
15.996	300.0	2171.5	10000	20.0	5.631	106.996	707.8	375.0	1.887	22940	4811.7100	0.1631	6014.6	6.0146E5	3.411E-3	0.3	1.8
17.000	300.0	2187.7	10000	20.0	5.645	108.000	713.1	375.0	1.901	23000	5063.0898	0.1635	6328.9	6.3289E5	3.411E-3	0.3	1.8
18.000	300.0	2175.5	10000	20.0	5.629	109.000	709.1	375.0	1.891	22940	5316.3599	0.1631	6645.5	6.6455E5	3.411E-3	0.3	1.8
19.000	300.0	2187.1	10000	20.0	5.625	110.000	712.9	375.0	1.901	22920	5691.3901	0.1630	7114.2	7.1142E5	3.411E-3	0.3	1.8
19.996	300.0	2184.8	10000	20.0	5.627	110.996	712.1	375.0	1.899	22930	5942.7002	0.1630	7428.4	7.4284E5	3.411E-3	0.3	1.8
20.992	300.0	2192.6	10000	20.0	5.649	111.992	714.7	375.0	1.906	23010	6320.8999	0.1637	7901.1	7.9011E5	3.411E-3	0.3	1.9
21.996	300.0	2196.3	10000	20.0	5.632	112.996	715.9	375.0	1.909	22950	6570.9600	0.1632	8213.7	8.2137E5	3.411E-3	0.4	1.9
23.000	300.0	2190.9	10000	20.0	5.637	114.000	714.1	375.0	1.904	22970	6823.8198	0.1633	8529.8	8.5298E5	3.411E-3	0.4	1.9
24.000	300.0	2199.5	10000	20.0	5.655	115.000	716.9	375.0	1.912	23040	7199.1899	0.1638	8999.0	8.9990E5	3.411E-3	0.4	1.9
25.032	300.0	2207.9	10000	20.0	5.650	116.032	719.7	375.0	1.919	23020	7450.6201	0.1637	9313.3	9.3133E5	3.411E-3	0.4	1.9
25.996	300.0	2194.3	10000	20.0	5.634	116.996	715.2	375.0	1.907	22950	7830.4702	0.1632	9788.1	9.7881E5	3.411E-3	0.4	1.9
27.000	300.0	2192.8	10000	20.0	5.635	118.000	714.7	375.0	1.906	22960	8080.0601	0.1633	10100	1.0100E6	3.411E-3	0.5	2.0
28.000	300.0	2210.2	10000	20.0	5.649	119.000	720.4	375.0	1.921	23020	8331.5195	0.1637	10414	1.0414E6	3.411E-3	0.5	2.0
29.000	300.0	2200.9	10000	20.0	5.631	120.000	717.4	375.0	1.913	22940	8708.3398	0.1632	10885	1.0885E6	3.411E-3	0.5	2.0
30.000	300.0	2189.6	10000	20.0	5.648	121.000	713.7	375.0	1.903	23010	8961.2100	0.1636	11202	1.1202E6	3.411E-3	0.5	2.0
31.000	300.0	2195.5	10000	20.0	5.646	122.000	715.6	375.0	1.908	23010	9213.0195	0.1636	11516	1.1516E6	3.411E-3	0.5	2.0
31.996	300.0	2215.6	10000	20.0	5.639	122.996	722.2	375.0	1.926	22980	9589.5303	0.1634	11987	1.1987E6	3.411E-3	0.5	2.0
33.000	300.0	2187.0	10000	20.0	5.640	124.000	712.8	375.0	1.901	22980	9839.1504	0.1634	12299	1.2299E6	3.411E-3	0.6	2.1
33.996	300.0	2188.0	10000	20.0	5.630	124.996	713.2	375.0	1.902	22940	10236.500	0.1631	12796	1.2796E6	3.411E-3	0.6	2.1
35.012	300.0	2219.4	10000	20.0	5.641	126.012	723.4	375.0	1.929	22980	10466.700	0.1635	13083	1.3083E6	3.411E-3	0.6	2.1
35.996	300.0	2199.3	10000	20.0	5.652	126.996	716.9	375.0	1.912	23030	10719.300	0.1638	13399	1.3399E6	3.411E-3	0.6	2.1
36.996	300.0	2202.8	10000	20.0	5.639	127.996	718.0	375.0	1.915	22980	11094.900	0.1634	13869	1.3869E6	3.411E-3	0.6	2.1
38.012	300.0	2190.7	10000	20.0	5.643	129.012	714.0	375.0	1.904	22990	11348.100	0.1635	14185	1.4185E6	3.411E-3	0.6	2.2
38.996	300.0	2197.3	10000	20.0	5.632	129.996	716.2	375.0	1.910	22950	11724.500	0.1632	14656	1.4656E6	3.411E-3	0.6	2.2
39.996	300.0	2198.1	10000	20.0	5.635	130.996	716.5	375.0	1.911	22960	11974.600	0.1633	14968	1.4968E6	3.411E-3	0.7	2.2
40.992	300.0	2202.5	10000	20.0	5.624	131.992	717.9	375.0	1.914	22910	12226.000	0.1629	15283	1.5283E6	3.411E-3	0.7	2.2
41.996	300.0	2199.6	10000	20.0	5.625	132.996	717.0	375.0	1.912	22920	12605.600	0.1629	15757	1.5757E6	3.411E-3	0.7	2.2
42.996	300.0	2192.8	10000	20.0	5.611	133.996	714.7	375.0	1.906	22860	12854.300	0.1626	16068	1.6068E6	3.411E-3	0.7	2.2
43.996	300.0	2193.3	10000	20.0	5.636	134.996	714.9	375.0	1.906	22960	13106.700	0.1633	16383	1.6383E6	3.411E-3	0.7	2.2
44.996	300.0	2215.6	10000	20.0	5.619	135.996	722.2	375.0	1.926	22890	13482.500	0.1628	16853	1.6853E6	3.411E-3	0.7	2.3
45.992	300.0	2197.0	10000	20.0	5.650	136.992	716.1	375.0	1.910	23020	13733.800	0.1637	17167	1.7167E6	3.411E-3	0.8	2.3
47.000	300.0	2198.3	10000	20.0	5.632	138.000	716.5	375.0	1.911	22950	14112.700	0.1632	17641	1.7641E6	3.411E-3	0.8	2.3
48.000	300.0	2195.5	10000	20.0	5.640	139.000	715.6	375.0	1.908	22980	14363.000	0.1634	17954	1.7954E6	3.411E-3	0.8	2.3
49.000	300.0	2196.7	10000	20.0	5.640	140.000	716.0	375.0	1.909	22980	14617.000	0.1634	18271	1.8271E6	3.411E-3	0.8	2.3
50.000	300.0	2195.7	10000	20.0	5.665	141.000	715.7	375.0	1.908	23080	14992.700	0.1641	18741	1.8741E6	3.411E-3	0.8	2.4
50.996	300.0	2176.7	10000	20.0	5.647	141.996	709.5	375.0	1.892	23010	15241.800	0.1636	19052	1.9052E6	3.411E-3	0.8	2.4
51.992	300.0	2200.8	10000	20.0	5.626	142.992	717.4	375.0	1.913	22920	15620.600	0.1630	19526	1.9526E6	3.411E-3	0.9	2.4
53.000	300.0	2200.3	10000	20.0	5.625	144.000	717.2	375.0	1.912	22920	15870.100	0.1630	19838	1.9838E6	3.411E-3	0.9	2.4
54.000	300.0	2191.4	10000	20.0	5.656	145.000	714.3	375.0	1.905	23040	16121.500	0.1639	20152	2.0152E6	3.411E-3	0.9	2.4
55.140	300.0	2221.8	10000	20.0	5.635	146.140	724.2	375.0	1.931	22960	16500.500	0.1633	20626	2.0626E6	3.411E-3	0.9	2.4
56.000	300.0	2185.0	10000	20.0	5.660	147.000	712.2	375.0	1.899	23060	16749.900	0.1640	20937	2.0937E6	3.411E-3	0.9	2.5
56.996	300.0	2192.5	10000	20.0	5.641	147.996	714.7	375.0	1.906	22980	17128.699	0.1634	21411	2.1411E6	3.411E-3	0.9	2.5
58.000	300.0	2206.3	10000	20.0	5.636	149.000	719.1	375.0	1.918	22960	17377.900	0.1633	21722	2.1722E6	3.411E-3	1.0	2.5
59.012	300.0	2208.9	10000	20.0	5.646	150.012	720.0	375.0	1.920	23000	17629.301	0.1636	22037	2.2037E6	3.411E-3	1.0	2.5
59.996	300.0	2190.1	10000	20.0	5.658	150.996	713.9	375.0	1.904	23050	18006.500	0.1639	22508	2.2508E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99200	297.4	2164.4	10000	20.0	5.637	151.992	705.5	371.7	1.898	22970	243.9310	0.1662	304.91	30491	3.411E-3	0.0	2.5
1.9960	291.4	2104.5	10000	20.0	5.653	152.996	686.0	364.2	1.883	23030	600.8900	0.1736	751.11	75111	3.411E-3	0.0	2.5
2.9960	287.3	2053.1	10000	20.0	5.656	153.996	669.2	359.2	1.863	23050	838.6910	0.1787	1048.4	1.0484E5	3.411E-3	0.0	2.6
4.0000	281.2	1991.8	10000	20.0	5.700	155.000	649.2	351.5	1.847	23230	1192.8800	0.1880	1491.1	1.4911E5	3.411E-3	0.1	2.6
4.9960	277.2	1937.5	10000	20.0	5.687	155.996	631.5	346.5	1.823	23170	1416.2500	0.1930	1770.3	1.7703E5	3.411E-3	0.1	2.6
5.9920	273.1	1895.1	10000	20.0	5.714	156.992	617.7	341.4	1.809	23280	1642.0900	0.1997	2052.6	2.0526E5	3.411E-3	0.1	2.6
6.9960	266.9	1813.6	10000	20.0	5.719	157.996	591.1	333.7	1.772	23300	1978.3700	0.2093	2473.0	2.4730E5	3.411E-3	0.1	2.6
7.9960	262.9	1802.6	10000	20.0	5.720	158.996	587.6	328.6	1.788	23310	2191.2300	0.2158	2739.0	2.7390E5	3.411E-3	0.1	2.6
8.9960	256.8	1709.0	10000	20.0	5.743	159.996	557.1	321.0	1.735	23400	2510.7600	0.2271	3138.5	3.1385E5	3.411E-3	0.1	2.7
9.9960	252.7	1684.9	10000	20.0	5.732	160.996	549.2	315.8	1.739	23360	2728.0400	0.2342	3410.1	3.4101E5	3.411E-3	0.2	2.7
10.996	248.5	1636.2	10000	20.0	5.751	161.996	533.3	310.6	1.717	23430	3033.7100	0.2428	3792.1	3.7921E5	3.411E-3	0.2	2.7
11.996	242.5	1590.8	10000	20.0	5.769	162.996	518.5	303.1	1.711	23500	3230.2600	0.2559	4037.8	4.0378E5	3.411E-3	0.2	2.7
12.992	238.3	1536.4	10000	20.0	5.792	163.992	500.8	297.9	1.681	23600	3430.7100	0.2658	4288.4	4.2884E5	3.411E-3	0.2	2.7
13.992	232.2	1474.0	10000	20.0	5.800	164.992	480.5	290.3	1.655	23630	3719.4299	0.2804	4649.3	4.6493E5	3.411E-3	0.2	2.7
14.996	228.2	1441.0	10000	20.0	5.803	165.996	469.7	285.2	1.647	23640	3915.7100	0.2907	4894.6	4.8946E5	3.411E-3	0.2	2.8
15.996	222.0	1372.6	10000	20.0	5.822	166.996	447.4	277.5	1.612	23720	4188.0298	0.3080	5235.0	5.2350E5	3.411E-3	0.3	2.8
16.996	217.8	1330.9	10000	20.0	5.829	167.996	433.8	272.3	1.593	23750	4369.2998	0.3203	5461.6	5.4616E5	3.411E-3	0.3	2.8
17.996	213.8	1289.5	10000	20.0	5.839	168.996	420.3	267.3	1.573	23790	4634.9800	0.3330	5793.7	5.7937E5	3.411E-3	0.3	2.8
18.992	207.6	1229.4	10000	20.0	5.856	169.992	400.7	259.5	1.544	23860	4807.1699	0.3542	6009.0	6.0090E5	3.411E-3	0.3	2.8
19.996	203.4	1193.0	10000	20.0	5.864	170.996	388.9	254.3	1.529	23890	4982.1201	0.3696	6227.7	6.2277E5	3.411E-3	0.3	2.8
20.992	197.3	1145.4	10000	20.0	5.868	171.992	373.3	246.7	1.514	23910	5226.9399	0.3930	6533.7	6.5337E5	3.411E-3	0.3	2.9
21.992	193.2	1094.4	10000	20.0	5.886	172.992	356.7	241.5	1.477	23980	5389.9902	0.4113	6737.5	6.7375E5	3.411E-3	0.4	2.9
22.992	189.0	1063.4	10000	20.0	5.887	173.992	346.6	236.2	1.467	23990	5551.2700	0.4299	6939.1	6.9391E5	3.411E-3	0.4	2.9
23.996	182.9	1005.9	10000	20.0	5.899	174.996	327.9	228.6	1.434	24040	5777.5400	0.4598	7221.9	7.2219E5	3.411E-3	0.4	2.9
24.996	178.8	974.28	10000	20.0	5.906	175.996	317.6	223.5	1.421	24060	5927.0098	0.4817	7408.8	7.4088E5	3.411E-3	0.4	2.9
26.000	172.5	921.54	10000	20.0	5.921	177.000	300.4	215.6	1.393	24130	6153.3999	0.5191	7691.8	7.6918E5	3.411E-3	0.4	3.0
26.992	168.4	879.82	10000	20.0	5.930	177.992	286.8	210.5	1.363	24160	6289.5298	0.5454	7861.9	7.8619E5	3.411E-3	0.4	3.0
27.992	164.3	849.97	10000	20.0	5.935	178.992	277.0	205.3	1.349	24180	6434.2202	0.5735	8042.8	8.0428E5	3.411E-3	0.5	3.0
28.996	157.9	796.08	10000	20.0	5.942	179.996	259.5	197.4	1.314	24210	6632.2900	0.6211	8290.4	8.2904E5	3.411E-3	0.5	3.0
29.996	153.9	771.14	10000	20.0	5.959	180.996	251.4	192.4	1.307	24280	6758.3198	0.6562	8447.9	8.4479E5	3.411E-3	0.5	3.0
30.996	147.7	721.97	10000	20.0	5.965	181.996	235.3	184.7	1.274	24300	6944.5298	0.7128	8680.7	8.6807E5	3.411E-3	0.5	3.0
31.992	143.5	679.76	10000	20.0	5.980	182.992	221.6	179.4	1.235	24360	7069.5698	0.7573	8837.0	8.8370E5	3.411E-3	0.5	3.0
33.000	139.2	655.13	10000	20.0	5.977	184.000	213.5	174.0	1.227	24350	7187.7998	0.8040	8984.8	8.9848E5	3.411E-3	0.6	3.1
34.044	133.1	606.62	10000	20.0	5.985	185.044	197.7	166.4	1.188	24390	7356.2500	0.8810	9195.3	9.1953E5	3.411E-3	0.6	3.1
34.992	128.9	583.10	10000	20.0	5.996	185.992	190.1	161.1	1.180	24430	7469.1201	0.9416	9336.4	9.3364E5	3.411E-3	0.6	3.1
35.992	124.6	546.93	10000	20.0	5.999	186.992	178.3	155.7	1.145	24440	7574.5000	1.008	9468.1	9.4681E5	3.411E-3	0.6	3.1
36.996	118.5	509.31	10000	20.0	6.010	187.996	166.0	148.1	1.121	24490	7724.0898	1.116	9655.1	9.6551E5	3.411E-3	0.6	3.1
38.000	114.3	478.42	10000	20.0	6.014	189.000	155.9	142.8	1.092	24500	7823.7202	1.201	9779.7	9.7797E5	3.411E-3	0.6	3.2
38.996	109.9	453.81	10000	20.0	6.019	189.996	147.9	137.3	1.077	24520	7923.3501	1.300	9904.2	9.9042E5	3.411E-3	0.6	3.2
40.100	103.6	408.40	10000	20.0	6.029	191.100	133.1	129.6	1.027	24560	8054.1299	1.463	10068	1.0068E6	3.411E-3	0.7	3.2
41.000	99.40	382.55	10000	20.0	6.030	192.000	124.7	124.3	1.004	24570	8141.2100	1.591	10177	1.0177E6	3.411E-3	0.7	3.2
42.100	92.84	345.12	10000	20.0	6.042	193.100	112.5	116.1	0.9693	24620	8265.9404	1.828	10332	1.0332E6	3.411E-3	0.7	3.2
42.996	88.77	320.78	10000	20.0	6.048	193.996	104.6	111.0	0.9423	24640	8340.0400	2.001	10425	1.0425E6	3.411E-3	0.7	3.2
43.996	84.51	295.78	10000	20.0	6.052	194.996	96.41	105.6	0.9126	24660	8414.5498	2.210	10518	1.0518E6	3.411E-3	0.7	3.2
44.992	80.03	270.91	10000	20.0	6.057	195.992	88.30	100.0	0.8827	24680	8488.9805	2.466	10611	1.0611E6	3.411E-3	0.7	3.3
45.996	73.42	239.19	10000	20.0	6.063	196.996	77.96	91.78	0.8495	24700	8588.1797	2.933	10735	1.0735E6	3.411E-3	0.8	3.3
46.996	69.12	218.13	10000	20.0	6.068	197.996	71.10	86.40	0.8229	24720	8650.0596	3.311	10813	1.0813E6	3.411E-3	0.8	3.3
47.996	64.54	192.19	10000	20.0	6.072	198.996	62.64	80.68	0.7765	24740	8711.8604	3.801	10890	1.0890E6	3.411E-3	0.8	3.3
48.996	59.88	172.27	10000	20.0	6.078	199.996	56.15	74.85	0.7502	24770	8767.4297	4.421	10959	1.0959E6	3.411E-3	0.8	3.3
50.000	55.64	154.22	10000	20.0	6.085	201.000	50.27	69.55	0.7228	24790	8816.8203	5.125	11021	1.1021E6	3.411E-3	0.8	3.4
50.992	51.06	132.71	10000	20.0	6.087	201.992	43.26	63.83	0.6777	24800	8866.0000	6.087	11083	1.1083E6	3.411E-3	0.8	3.4
52.000	43.70	103.52	10000	20.0	6.094	203.000	33.74	54.62	0.6177	24830	8933.9600	8.322	11167	1.1167E6	3.411E-3	0.9	3.4
53.068	39.30	87.103	10000	20.0	6.098	204.068	28.39	49.12	0.5780	24840	8970.2500	10.30	11213	1.1213E6	3.411E-3	0.9	3.4
54.004	34.38	70.131	10000	20.0	6.098	205.004	22.86	42.97	0.5320	24850	9006.8398	13.46	11259	1.1259E6	3.411E-3	0.9	3.4
55.140	29.20	55.790	10000	20.0	6.097	206.140	18.18	36.50	0.4982	24840	9036.9600	18.65	11296	1.1296E6	3.411E-3	0.9	3.4
55.996	24.75	41.696	10000	20.0	6.100	206.996	13.59	30.94	0.4393	24850	9061.2197	25.97	11327	1.1327E6	3.411E-3	0.9	3.4
56.996	19.39	28.589	10000	20.0	6.104	207.996	9.319	24.24	0.3844	24870	9084.7305	42.32	11356	1.1356E6	3.411E-3	0.9	3.5
57.992	16.15	21.477	10000	20.0	6.106	208.992	7.000	20.19	0.3468	24880	9096.0303	61.06	11370	1.1370E6	3.411E-3	1.0	3.5
58.992	10.95	11.805	10000	20.0	6.108	209.992	3.848	13.69	0.2812	24890	9107.5000	132.9	11384	1.1384E6	3.411E-3	1.0	3.5
60.068	5.206	2.8569	10000	20.0	6.106	211.068	0.9312	6.508	0.1431	24880	9115.2998	587.5	11394	1.1394E6	3.411E-3	1.0	3.5

